Information card for entry 7048115

Structure parameters

• Chemical name: bis[N,N-diethyl-N`-2-naphthoylthioureato] lead(II)
• Formula: C32 H34 N4 O2 Pb S2
• Calculated formula: C32 H34 N4 O2 Pb S2
• Title of publication: Full compositional control of PbS_xSe_1-x thin films by the use of acylchalcogourato lead(ii) complexes as precursors for AACVD.
• Authors of publication: Ezenwa, Tagbo Emmanuel; McNaughter, Paul D.; Raftery, James; Lewis, David J.; O'Brien, Paul
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2018
• Journal volume: 47
• Journal issue: 47
• Pages of publication: 16938 - 16943
• a: 10.697 ± 0.0003 Å
• b: 10.8385 ± 0.0004 Å
• c: 26.5087 ± 0.0009 Å
• α: 90°
• β: 98.916 ± 0.002°
• γ: 90°
• Cell volume: 3036.27 ± 0.18 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0388
• Residual factor for significantly intense reflections: 0.0348
• Weighted residual factors for significantly intense reflections: 0.0916
• Weighted residual factors for all reflections included in the refinement: 0.0938
• Goodness-of-fit parameter for all reflections included in the refinement: 1.151
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No