Crystallography Open Database

Information card for entry 7048300

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Coordinates	7048300.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H50 O22 Si12
Calculated formula	C16 H50 O22 Si12
Title of publication	Synthesis and crystal structure of double-three ring (D3R)-type cage siloxanes modified with dimethylsilanol groups.
Authors of publication	Sato, Naoto; Tochigi, Kazuma; Kuroda, Yoshiyuki; Wada, Hiroaki; Shimojima, Atsushi; Kuroda, Kazuyuki
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	6
Pages of publication	1969 - 1975
a	17.2739 ± 0.0005 Å
b	10.8748 ± 0.0003 Å
c	23.2168 ± 0.0007 Å
α	90°
β	90.452 ± 0.006°
γ	90°
Cell volume	4361.1 ± 0.2 Å³
Cell temperature	123 K
Ambient diffraction temperature	123 K
Number of distinct elements	4
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.1029
Residual factor for significantly intense reflections	0.062
Weighted residual factors for significantly intense reflections	0.1204
Weighted residual factors for all reflections included in the refinement	0.135
Goodness-of-fit parameter for all reflections included in the refinement	1.016
Diffraction radiation wavelength	1.54187 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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