Information card for entry 7048303

Structure parameters

• Formula: C30 H28 Cl N2 O P Pd
• Calculated formula: C30 H28 Cl N2 O P Pd
• Title of publication: Synthesis of nickel and palladium complexes with diarylamido-based unsymmetrical pincer ligands and application for norbornene polymerization.
• Authors of publication: Liu, Hui; Yuan, Haibin; Shi, Xiaochao
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 2
• Pages of publication: 609 - 617
• a: 9.347 ± 0.005 Å
• b: 10.065 ± 0.006 Å
• c: 28.656 ± 0.016 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2696 ± 3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0184
• Residual factor for significantly intense reflections: 0.0178
• Weighted residual factors for significantly intense reflections: 0.0444
• Weighted residual factors for all reflections included in the refinement: 0.0446
• Goodness-of-fit parameter for all reflections included in the refinement: 1.199
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No