Information card for entry 7048365

Structure parameters

• Formula: C43 H60 F3 Li N4.5 O2 P2 Pd S
• Calculated formula: C43 H60 F3 Li N4.5 O2 P2 Pd S
• Title of publication: Highly efficient palladium-catalysed carbon dioxide hydrosilylation employing PMP ligands.
• Authors of publication: Steinhoff, Patrick; Paul, Melanie; Schroers, Julian P.; Tauchert, Michael E.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 3
• Pages of publication: 1017 - 1022
• a: 14.6156 ± 0.0008 Å
• b: 19.4178 ± 0.001 Å
• c: 40.0329 ± 0.0019 Å
• α: 90°
• β: 99.083 ± 0.001°
• γ: 90°
• Cell volume: 11219 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0907
• Residual factor for significantly intense reflections: 0.0784
• Weighted residual factors for significantly intense reflections: 0.1889
• Weighted residual factors for all reflections included in the refinement: 0.1976
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No