Information card for entry 7048595

Structure parameters

• Formula: C24 H25 Cl Ge O3 S2
• Calculated formula: C24 H25 Cl Ge O3 S2
• Title of publication: A non-symmetric sulfur-based O,C,O-chelating pincer ligand leading to chiral germylene and stannylene.
• Authors of publication: Deak, Noemi; Thillaye du Boullay, Olivier; Moraru, Ionut-Tudor; Mallet-Ladeira, Sonia; Madec, David; Nemes, Gabriela
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 7
• Pages of publication: 2399 - 2406
• a: 9.4696 ± 0.0007 Å
• b: 9.6861 ± 0.0007 Å
• c: 13.773 ± 0.001 Å
• α: 105.093 ± 0.002°
• β: 90.07 ± 0.002°
• γ: 94.398 ± 0.002°
• Cell volume: 1215.84 ± 0.15 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0444
• Residual factor for significantly intense reflections: 0.0333
• Weighted residual factors for significantly intense reflections: 0.0829
• Weighted residual factors for all reflections included in the refinement: 0.0883
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No