Information card for entry 7048892

Structure parameters

• Common name: [Li2(N3Dmp2)(n-Bu)]
• Formula: C52 H59 Li2 N3
• Calculated formula: C52 H59 Li2 N3
• Title of publication: Structural diversity in a homologous series of donor free alkali metal complexes bearing a sterically demanding triazenide.
• Authors of publication: McKay, Alasdair I.; Cole, Marcus L.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 9
• Pages of publication: 2948 - 2952
• a: 11.4916 ± 0.0004 Å
• b: 30.8596 ± 0.0012 Å
• c: 13.3457 ± 0.0005 Å
• α: 90°
• β: 110.931 ± 0.002°
• γ: 90°
• Cell volume: 4420.4 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150.15 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0936
• Residual factor for significantly intense reflections: 0.0558
• Weighted residual factors for significantly intense reflections: 0.1299
• Weighted residual factors for all reflections included in the refinement: 0.1466
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No