Information card for entry 7048914

Structure parameters

• Formula: C16 H23 F3 Ge N2 O3 S
• Calculated formula: C16 H23 F3 Ge N2 O3 S
• Title of publication: Ge(ii) cation catalyzed hydroboration of aldehydes and ketones.
• Authors of publication: Sinhababu, Soumen; Singh, Dharmendra; Sharma, Mahendra Kumar; Siwatch, Rahul Kumar; Mahawar, Pritam; Nagendran, Selvarajan
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 13
• Pages of publication: 4094 - 4100
• a: 15.057 ± 0.003 Å
• b: 16.433 ± 0.003 Å
• c: 16.648 ± 0.003 Å
• α: 90°
• β: 93.621 ± 0.004°
• γ: 90°
• Cell volume: 4111 ± 1.3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0714
• Residual factor for significantly intense reflections: 0.0446
• Weighted residual factors for significantly intense reflections: 0.1013
• Weighted residual factors for all reflections included in the refinement: 0.1103
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No