Information card for entry 7048928

Structure parameters

• Formula: C6 H20 N4 S3 Sb V
• Calculated formula: C6.005 H20 N4 S3 Sb V
• Title of publication: A series of new vanadium(iii) chalcogenido-antimonates: an unusual seven-coordinate nitro-selenidovanadium(iii) complex.
• Authors of publication: Luo, Hai-Ying; Zhou, Jian; Zou, Hua-Hong
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 9
• Pages of publication: 3090 - 3097
• a: 6.468 ± 0.004 Å
• b: 17.708 ± 0.009 Å
• c: 13.526 ± 0.007 Å
• α: 90°
• β: 108.5 ± 0.016°
• γ: 90°
• Cell volume: 1469.1 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0469
• Residual factor for significantly intense reflections: 0.0372
• Weighted residual factors for significantly intense reflections: 0.1029
• Weighted residual factors for all reflections included in the refinement: 0.1131
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No