Information card for entry 7048930

Structure parameters

• Formula: C16 H57 N13 O Sb2 Se8 V2
• Calculated formula: C16 H57 N13 O Sb2 Se8 V2
• Title of publication: A series of new vanadium(iii) chalcogenido-antimonates: an unusual seven-coordinate nitro-selenidovanadium(iii) complex.
• Authors of publication: Luo, Hai-Ying; Zhou, Jian; Zou, Hua-Hong
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 9
• Pages of publication: 3090 - 3097
• a: 8.984 ± 0.008 Å
• b: 16.043 ± 0.016 Å
• c: 28.431 ± 0.01 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4098 ± 6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0628
• Residual factor for significantly intense reflections: 0.0366
• Weighted residual factors for significantly intense reflections: 0.0543
• Weighted residual factors for all reflections included in the refinement: 0.0597
• Goodness-of-fit parameter for all reflections included in the refinement: 0.986
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No