Information card for entry 7049049

Structure parameters

• Formula: C82 H72 Fe8 Ge6 O14
• Calculated formula: C82 H72 Fe8 Ge6 O14
• Title of publication: On the reaction of GeCl2·Dioxane with KFeCp(CO)2: Isolation and characterization of novel bimetallic clusters
• Authors of publication: Schnepf, Andreas; Schrenk, Claudio; Preißing, Lars
• Journal of publication: Dalton Transactions
• Year of publication: 2019
• a: 20.9394 ± 0.001 Å
• b: 20.9394 ± 0.001 Å
• c: 17.7553 ± 0.0019 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7785 ± 1 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 5
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.0776
• Residual factor for significantly intense reflections: 0.0497
• Weighted residual factors for significantly intense reflections: 0.1301
• Weighted residual factors for all reflections included in the refinement: 0.154
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No