Information card for entry 7049101

Structure parameters

• Formula: C33 H27 Cl1.77 I0.23 Sb
• Calculated formula: C33 H27 Cl1.7742 I0.2258 Sb
• Title of publication: Increasing steric demand through flexible bulk - primary phosphanes with 2,6-bis(benzhydryl)phenyl backbones.
• Authors of publication: Bresien, Jonas; Goicoechea, Jose M.; Hinz, Alexander; Scharnhölz, Moritz T; Schulz, Axel; Suhrbier, Tim; Villinger, Alexander
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 11
• Pages of publication: 3786 - 3794
• a: 9.5535 ± 0.0009 Å
• b: 12.4822 ± 0.0012 Å
• c: 13.5312 ± 0.0013 Å
• α: 104.561 ± 0.004°
• β: 106.008 ± 0.004°
• γ: 109.385 ± 0.004°
• Cell volume: 1354.4 ± 0.2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0527
• Residual factor for significantly intense reflections: 0.0363
• Weighted residual factors for significantly intense reflections: 0.07
• Weighted residual factors for all reflections included in the refinement: 0.0765
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No