Information card for entry 7049118

Structure parameters

• Formula: C52 H59 F24 N19 O P4 Rh2
• Calculated formula: C52 H59 F24 N19 O P4 Rh2
• Title of publication: Unbridged Rh(ii)-Rh(ii) complexes of N-heterocyclic carbenes and reactions with O₂ to form dirhodium(μ-η¹:η¹-O₂) complexes.
• Authors of publication: Yi, Xiaofei; Liu, Bin; Chen, Kai; Chen, Wei; Chen, Wanzhi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 12
• Pages of publication: 3835 - 3839
• a: 19.0638 ± 0.0006 Å
• b: 15.4706 ± 0.0005 Å
• c: 26.2772 ± 0.0009 Å
• α: 90°
• β: 103.647 ± 0.003°
• γ: 90°
• Cell volume: 7531.1 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1063
• Residual factor for significantly intense reflections: 0.071
• Weighted residual factors for significantly intense reflections: 0.186
• Weighted residual factors for all reflections included in the refinement: 0.2198
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No