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Information card for entry 7049181
Preview
Coordinates | 7049181.cif |
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Original paper (by DOI) | HTML |
Chemical name | (bispentamethylcyclopentadienylnickel)-1,2,3,5,6,7-hexamethylbicyclooct[3.3.0]ane |
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Formula | C34 H48 Ni2 |
Calculated formula | C34 H48 Ni2 |
Title of publication | Synthesis, characterisation and redox properties of anti-bimetallic permethylpentalene complexes. |
Authors of publication | Binding, Samantha C.; Green, Jennifer C.; Turner, Zoë R; Buffet, Jean-Charles; O'Hare, Dermot |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2019 |
Journal volume | 48 |
Journal issue | 13 |
Pages of publication | 4263 - 4273 |
a | 8.8663 ± 0.0003 Å |
b | 15.1452 ± 0.0007 Å |
c | 11.5069 ± 0.0004 Å |
α | 90° |
β | 104.974 ± 0.003° |
γ | 90° |
Cell volume | 1492.7 ± 0.1 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 3 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0656 |
Residual factor for significantly intense reflections | 0.0395 |
Weighted residual factors for all reflections | 0.1066 |
Weighted residual factors for significantly intense reflections | 0.0838 |
Weighted residual factors for all reflections included in the refinement | 0.1066 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.948 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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