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Information card for entry 7049192
Preview
Coordinates | 7049192.cif |
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Original paper (by DOI) | HTML |
Formula | C24 H20 B F10 N Si |
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Calculated formula | C24 H20 B F10 N Si |
Title of publication | Consecutive intermolecular 1,1-carboboration reactions of Me<sub>3</sub>Si-substituted alkynes with the halogeno-B(C<sub>6</sub>F<sub>5</sub>)<sub>2</sub> reagents. |
Authors of publication | Škoch, Karel; Pauly, Christophe; Daniliuc, Constantin G.; Bergander, Klaus; Kehr, Gerald; Erker, Gerhard |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2019 |
Journal volume | 48 |
Journal issue | 15 |
Pages of publication | 4837 - 4845 |
a | 10.7974 ± 0.0003 Å |
b | 11.4497 ± 0.0004 Å |
c | 13.2136 ± 0.0006 Å |
α | 81.389 ± 0.001° |
β | 70.405 ± 0.001° |
γ | 62.3 ± 0.002° |
Cell volume | 1362.54 ± 0.09 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0784 |
Residual factor for significantly intense reflections | 0.0587 |
Weighted residual factors for significantly intense reflections | 0.1201 |
Weighted residual factors for all reflections included in the refinement | 0.1331 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.072 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7049192.html
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