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Information card for entry 7049194
Preview
Coordinates | 7049194.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C13 H3 B F10 |
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Calculated formula | C13 H3 B F10 |
Title of publication | Consecutive intermolecular 1,1-carboboration reactions of Me<sub>3</sub>Si-substituted alkynes with the halogeno-B(C<sub>6</sub>F<sub>5</sub>)<sub>2</sub> reagents. |
Authors of publication | Škoch, Karel; Pauly, Christophe; Daniliuc, Constantin G.; Bergander, Klaus; Kehr, Gerald; Erker, Gerhard |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2019 |
Journal volume | 48 |
Journal issue | 15 |
Pages of publication | 4837 - 4845 |
a | 5.2909 ± 0.0004 Å |
b | 9.4999 ± 0.0011 Å |
c | 26.104 ± 0.003 Å |
α | 90° |
β | 90.161 ± 0.008° |
γ | 90° |
Cell volume | 1312.1 ± 0.2 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.064 |
Residual factor for significantly intense reflections | 0.047 |
Weighted residual factors for significantly intense reflections | 0.1139 |
Weighted residual factors for all reflections included in the refinement | 0.1269 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.08 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7049194.html
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Users of the data should acknowledge the original authors of the
structural data.