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Information card for entry 7049199
Preview
Coordinates | 7049199.cif |
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Original paper (by DOI) | HTML |
Formula | C28 H25 B Cl F10 N Si |
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Calculated formula | C28 H25 B Cl F10 N Si |
Title of publication | Consecutive intermolecular 1,1-carboboration reactions of Me<sub>3</sub>Si-substituted alkynes with the halogeno-B(C<sub>6</sub>F<sub>5</sub>)<sub>2</sub> reagents. |
Authors of publication | Škoch, Karel; Pauly, Christophe; Daniliuc, Constantin G.; Bergander, Klaus; Kehr, Gerald; Erker, Gerhard |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2019 |
Journal volume | 48 |
Journal issue | 15 |
Pages of publication | 4837 - 4845 |
a | 12.1069 ± 0.0005 Å |
b | 16.3988 ± 0.0006 Å |
c | 19.2005 ± 0.0008 Å |
α | 113.692 ± 0.001° |
β | 98.198 ± 0.002° |
γ | 100.822 ± 0.001° |
Cell volume | 3326.4 ± 0.2 Å3 |
Cell temperature | 102 ± 2 K |
Ambient diffraction temperature | 102 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0704 |
Residual factor for significantly intense reflections | 0.0437 |
Weighted residual factors for significantly intense reflections | 0.09 |
Weighted residual factors for all reflections included in the refinement | 0.0983 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.021 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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