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Information card for entry 7049201
Preview
Coordinates | 7049201.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C36 H50 B2 F10 O3 Si4 |
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Calculated formula | C36 H50 B2 F10 O3 Si4 |
Title of publication | Consecutive intermolecular 1,1-carboboration reactions of Me<sub>3</sub>Si-substituted alkynes with the halogeno-B(C<sub>6</sub>F<sub>5</sub>)<sub>2</sub> reagents. |
Authors of publication | Škoch, Karel; Pauly, Christophe; Daniliuc, Constantin G.; Bergander, Klaus; Kehr, Gerald; Erker, Gerhard |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2019 |
Journal volume | 48 |
Journal issue | 15 |
Pages of publication | 4837 - 4845 |
a | 23.7133 ± 0.0005 Å |
b | 7.5887 ± 0.0002 Å |
c | 25.2856 ± 0.0006 Å |
α | 90° |
β | 114.834 ± 0.001° |
γ | 90° |
Cell volume | 4129.46 ± 0.17 Å3 |
Cell temperature | 112 ± 2 K |
Ambient diffraction temperature | 112 ± 2 K |
Number of distinct elements | 6 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0386 |
Residual factor for significantly intense reflections | 0.033 |
Weighted residual factors for significantly intense reflections | 0.0797 |
Weighted residual factors for all reflections included in the refinement | 0.083 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.051 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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