Information card for entry 7049285

Structure parameters

• Formula: C46 H42 Cl10 F6 Ge2 N2 O6 P2 S2
• Calculated formula: C46 H42 Cl10 F6 Ge2 N2 O6 P2 S2
• Title of publication: Stabilization of bis(chlorogermyliumylidene)s within bifunctional PNNP ligand frameworks and their reactivity studies.
• Authors of publication: Sahoo, Padmini; Raut, Ravindra K.; Maurya, Devesh; Kumar, Vikas; Rani, Pooja; Gonnade, Rajesh G.; Majumdar, Moumita
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 21
• Pages of publication: 7344 - 7351
• a: 11.033 ± 0.001 Å
• b: 12.4374 ± 0.0011 Å
• c: 13.1345 ± 0.0012 Å
• α: 62.303 ± 0.003°
• β: 71.71 ± 0.003°
• γ: 64.929 ± 0.003°
• Cell volume: 1430 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0443
• Residual factor for significantly intense reflections: 0.0388
• Weighted residual factors for significantly intense reflections: 0.1026
• Weighted residual factors for all reflections included in the refinement: 0.1055
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No