Information card for entry 7049338

Structure parameters

• Formula: C98 H216 O36 Si8 Yb4
• Calculated formula: C98 H216 O36 Si8 Yb4
• Title of publication: Carbon dioxide reduction by dinuclear Yb(ii) and Sm(ii) complexes supported by siloxide ligands.
• Authors of publication: Willauer, Aurélien R; Toniolo, Davide; Fadaei-Tirani, Farzaneh; Yang, Yan; Laurent, Maron; Mazzanti, Marinella
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 18
• Pages of publication: 6100 - 6110
• a: 13.1265 ± 0.0002 Å
• b: 15.6137 ± 0.0003 Å
• c: 18.8708 ± 0.0004 Å
• α: 72.6073 ± 0.0017°
• β: 80.2421 ± 0.0015°
• γ: 79.3717 ± 0.0013°
• Cell volume: 3600.42 ± 0.12 ų
• Cell temperature: 140.01 ± 0.1 K
• Ambient diffraction temperature: 140.01 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0228
• Residual factor for significantly intense reflections: 0.0215
• Weighted residual factors for significantly intense reflections: 0.0541
• Weighted residual factors for all reflections included in the refinement: 0.0548
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No