Information card for entry 7049347

Structure parameters

• Formula: C46 H57 Co N2 P Si
• Calculated formula: C46 H57 Co N2 P Si
• Title of publication: Cyclometallation reactions of a three-coordinate cobalt(i) complex bearing a nonsymmetric N-heterocyclic carbene ligand.
• Authors of publication: Gao, Yafei; Chen, Qi; Leng, Xuebing; Deng, Liang
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 26
• Pages of publication: 9676 - 9683
• a: 11.7137 ± 0.0014 Å
• b: 11.7791 ± 0.0013 Å
• c: 17.1943 ± 0.0019 Å
• α: 73.315 ± 0.002°
• β: 81.611 ± 0.002°
• γ: 62.113 ± 0.002°
• Cell volume: 2008.4 ± 0.4 ų
• Cell temperature: 130 K
• Ambient diffraction temperature: 130 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0991
• Residual factor for significantly intense reflections: 0.0569
• Weighted residual factors for significantly intense reflections: 0.1338
• Weighted residual factors for all reflections included in the refinement: 0.1602
• Goodness-of-fit parameter for all reflections included in the refinement: 0.897
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No