Information card for entry 7049351

Structure parameters

• Formula: C16 H44 Al Cl N2 O Si4
• Calculated formula: C16 H44 Al Cl N2 O Si4
• Title of publication: Grafting of a new bis-silylamido aluminum species on silica: insight from solid-state NMR into interactions with the surface.
• Authors of publication: Vancompernolle, Tom; Merle, Nicolas; Capet, Frédéric; Del Rosal, Iker; Laurent, Maron; Delevoye, Laurent; Pourpoint, Frédérique; Gauvin, Régis M
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 16
• Pages of publication: 5243 - 5252
• a: 8.3419 ± 0.0004 Å
• b: 11.3931 ± 0.0005 Å
• c: 15.5621 ± 0.0007 Å
• α: 104.962 ± 0.002°
• β: 93.099 ± 0.002°
• γ: 109.088 ± 0.002°
• Cell volume: 1334.69 ± 0.11 ų
• Cell temperature: 100.15 K
• Ambient diffraction temperature: 100.15 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.038
• Residual factor for significantly intense reflections: 0.0294
• Weighted residual factors for significantly intense reflections: 0.074
• Weighted residual factors for all reflections included in the refinement: 0.079
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No