Information card for entry 7049376
| Formula |
C33 H29 O6 |
| Calculated formula |
C33 H25 O6 |
| Title of publication |
Cyclotrimerization of alkynes catalyzed by a self-supported cyclic tri-nuclear nickel(0) complex with α-diimine ligands. |
| Authors of publication |
Shen, Lingyi; Zhao, Yanxia; Luo, Qiong; Li, Qian-Shu; Liu, Bin; Redshaw, Carl; Wu, Biao; Yang, Xiao-Juan |
| Journal of publication |
Dalton transactions (Cambridge, England : 2003) |
| Year of publication |
2019 |
| Journal volume |
48 |
| Journal issue |
14 |
| Pages of publication |
4643 - 4649 |
| a |
22.007 ± 0.007 Å |
| b |
12.847 ± 0.007 Å |
| c |
11.149 ± 0.005 Å |
| α |
90° |
| β |
112.394 ± 0.008° |
| γ |
90° |
| Cell volume |
2914 ± 2 Å3 |
| Cell temperature |
153 ± 2 K |
| Ambient diffraction temperature |
153 ± 2 K |
| Number of distinct elements |
3 |
| Space group number |
9 |
| Hermann-Mauguin space group symbol |
C 1 c 1 |
| Hall space group symbol |
C -2yc |
| Residual factor for all reflections |
0.0928 |
| Residual factor for significantly intense reflections |
0.062 |
| Weighted residual factors for significantly intense reflections |
0.1312 |
| Weighted residual factors for all reflections included in the refinement |
0.1446 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.12 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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