Information card for entry 7049383

Structure parameters

• Chemical name: [Pd{?1-NIM-[N-(diphenylboryl)-2-benzoylpyridinketimine]}Cl(C3H5)]
• Formula: C55 H49 B2 Cl5 N4 Pd2
• Calculated formula: C55 H49 B2 Cl5 N4 Pd2
• Title of publication: Synthesis, structure and palladium coordination of ambiphilic, pyridine- and phosphine-tethered N-boryl imine ligands.
• Authors of publication: Lorenzini, Fabio; Lagueux-Tremblay, Pierre-Louis; Kayser, Laure V.; Anderson, Ethan; Arndtsen, Bruce A.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 17
• Pages of publication: 5766 - 5772
• a: 9.1405 ± 0.0004 Å
• b: 16.5696 ± 0.0008 Å
• c: 18.1527 ± 0.0009 Å
• α: 84.192 ± 0.001°
• β: 85.267 ± 0.001°
• γ: 78.666 ± 0.001°
• Cell volume: 2676.3 ± 0.2 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0515
• Residual factor for significantly intense reflections: 0.0368
• Weighted residual factors for significantly intense reflections: 0.0855
• Weighted residual factors for all reflections included in the refinement: 0.0945
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No