Information card for entry 7049409

Structure parameters

• Formula: C33.77 H33.53 Au Cl3.53 N3 O
• Calculated formula: C33.767 H33.534 Au Cl3.534 N3 O
• Title of publication: Direct intramolecular carbon(sp²)-nitrogen(sp²) reductive elimination from gold(iii).
• Authors of publication: Kim, Jong Hyun; Mertens, R. Tyler; Agarwal, Amal; Parkin, Sean; Berger, Gilles; Awuah, Samuel G.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 18
• Pages of publication: 6273 - 6282
• a: 11.3471 ± 0.0003 Å
• b: 13.4416 ± 0.0005 Å
• c: 21.6337 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3299.64 ± 0.19 ų
• Cell temperature: 90 ± 0.2 K
• Ambient diffraction temperature: 90 ± 0.2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0413
• Residual factor for significantly intense reflections: 0.0379
• Weighted residual factors for significantly intense reflections: 0.0916
• Weighted residual factors for all reflections included in the refinement: 0.0928
• Goodness-of-fit parameter for all reflections included in the refinement: 1.208
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No