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Information card for entry 7049495
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Coordinates | 7049495.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C52 H74 F8 N2 Ni O P2 |
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Calculated formula | C52 H74 F8 N2 Ni O P2 |
Title of publication | C-F activation of perfluorophenazine at nickel: selectivity and mechanistic investigations. |
Authors of publication | Torres, Òscar; Pfister, Nils; Braun, Thomas; Wittwer, Philipp |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2019 |
Journal volume | 48 |
Journal issue | 18 |
Pages of publication | 6153 - 6161 |
a | 11.9941 ± 0.0006 Å |
b | 13.6197 ± 0.0007 Å |
c | 17.6604 ± 0.001 Å |
α | 72.302 ± 0.002° |
β | 72.776 ± 0.002° |
γ | 66.228 ± 0.002° |
Cell volume | 2464.9 ± 0.2 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0718 |
Residual factor for significantly intense reflections | 0.0555 |
Weighted residual factors for significantly intense reflections | 0.1452 |
Weighted residual factors for all reflections included in the refinement | 0.1571 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.034 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7049495.html
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Users of the data should acknowledge the original authors of the
structural data.