Information card for entry 7049591

Structure parameters

• Formula: C30 H21 N2 O7 P W
• Calculated formula: C30 H21 N2 O7 P W
• Title of publication: An approach to 7-aza-1-phosphanorbornane complexes: strain promoted rearrangement of 1-iminylphosphirane complexes and cycloaddition with olefins.
• Authors of publication: Xu, Yang; Wang, Min; Wei, Donghui; Tian, Rongqiang; Duan, Zheng; Mathey, François
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 17
• Pages of publication: 5523 - 5526
• a: 20.6471 ± 0.0006 Å
• b: 11.903 ± 0.0003 Å
• c: 11.9069 ± 0.0004 Å
• α: 90°
• β: 92.994 ± 0.003°
• γ: 90°
• Cell volume: 2922.27 ± 0.15 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0535
• Residual factor for significantly intense reflections: 0.0357
• Weighted residual factors for significantly intense reflections: 0.052
• Weighted residual factors for all reflections included in the refinement: 0.0584
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No