Information card for entry 7049662

Structure parameters

• Formula: C16 H8 F2 Mo O8 P2
• Calculated formula: C16 H8 F2 Mo O8 P2
• Title of publication: Ring size effects in cyclic fluorophosphites: ligands that span the bonding space between phosphites and PF3
• Authors of publication: Miles-Hobbs, Alexandra M.; Hunt, Eliza; Pringle, Paul. G.; Sparkes, Hazel A.
• Journal of publication: Dalton Transactions
• Year of publication: 2019
• a: 13.9152 ± 0.0003 Å
• b: 20.666 ± 0.0004 Å
• c: 6.4314 ± 0.0001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1849.49 ± 0.06 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0232
• Residual factor for significantly intense reflections: 0.0205
• Weighted residual factors for significantly intense reflections: 0.0466
• Weighted residual factors for all reflections included in the refinement: 0.0478
• Goodness-of-fit parameter for all reflections included in the refinement: 1.109
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No