Information card for entry 7049724

Structure parameters

• Formula: C85 H87 Ge5 Mo32 N17 O96 Zn
• Calculated formula: C70 H70 Ge5 Mo32 N14 O96 Zn
• Title of publication: POM-FLPs: [Mo]_n-polyoxometalate bifunctional catalysis by [Mo]_n-O_m Lewis pairs frustrated by triangular Mo^IV-Mo^IV bonds.
• Authors of publication: Luo, Benlong; Xu, Li
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 20
• Pages of publication: 6892 - 6898
• a: 22.763 ± 0.004 Å
• b: 13.703 ± 0.002 Å
• c: 27.665 ± 0.005 Å
• α: 90°
• β: 112.075 ± 0.003°
• γ: 90°
• Cell volume: 7997 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0731
• Residual factor for significantly intense reflections: 0.0643
• Weighted residual factors for significantly intense reflections: 0.1198
• Weighted residual factors for all reflections included in the refinement: 0.1234
• Goodness-of-fit parameter for all reflections included in the refinement: 1.29
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No