Crystallography Open Database

Information card for entry 7049856

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Coordinates	7049856.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C119 H119.99 Ge2 N10 O0.5 Pd6
Calculated formula	C119 H120.585 Ge2 N10 O0.5 Pd6
Title of publication	Bimolecular fusion of [Pd<sub>3</sub>(μ-CN-C<sub>6</sub>H<sub>3</sub>Me<sub>2</sub>-2,6)<sub>3</sub>(CN-C<sub>6</sub>H<sub>3</sub>Me<sub>2</sub>-2,6)<sub>3</sub>] induced by Ph<sub>2</sub>GeH<sub>2</sub>: formation of the redox-active Pd<sub>6</sub>Ge<sub>2</sub> complex.
Authors of publication	Koizumi, Take-Aki; Tanaka, Kimiya; Tsuchido, Yoshitaka; Tanabe, Makoto; Ide, Tomohito; Osakada, Kohtaro
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	22
Pages of publication	7541 - 7545
a	15.2741 ± 0.0001 Å
b	16.0021 ± 0.0001 Å
c	26.7383 ± 0.0003 Å
α	83.018 ± 0.001°
β	74.7 ± 0.001°
γ	62.547 ± 0.001°
Cell volume	5593.82 ± 0.1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	1
Hermann-Mauguin space group symbol	P 1
Hall space group symbol	P 1
Residual factor for all reflections	0.0287
Residual factor for significantly intense reflections	0.0278
Weighted residual factors for significantly intense reflections	0.07
Weighted residual factors for all reflections included in the refinement	0.0705
Goodness-of-fit parameter for all reflections included in the refinement	1.057
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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