Information card for entry 7049896

Structure parameters

• Formula: C52 H54 B2 N12 O4 Se2 Si W2
• Calculated formula: C52 H54 B2 N12 O4 Se2 Si W2
• Title of publication: Alkynylselenolatoalkylidynes (L_nM[triple bond, length as m-dash]C-Se-C[triple bond, length as m-dash]CR) as building blocks for mixed metal/main-group extended frameworks.
• Authors of publication: Frogley, Benjamin J.; Genet, Tobias L.; Hill, Anthony F.; Onn, Chee S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2019
• Journal volume: 48
• Journal issue: 22
• Pages of publication: 7632 - 7643
• a: 14.611 ± 0.008 Å
• b: 15.247 ± 0.003 Å
• c: 15.864 ± 0.003 Å
• α: 74.469 ± 0.003°
• β: 65.54 ± 0.015°
• γ: 89.467 ± 0.01°
• Cell volume: 3078.6 ± 1.9 ų
• Cell temperature: 100.409 ± 0.0002 K
• Ambient diffraction temperature: 100.409 ± 0.0002 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1564
• Residual factor for significantly intense reflections: 0.0623
• Weighted residual factors for significantly intense reflections: 0.1378
• Weighted residual factors for all reflections included in the refinement: 0.1757
• Goodness-of-fit parameter for all reflections included in the refinement: 0.88
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No