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Information card for entry 7049938
Preview
Coordinates | 7049938.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C91 H82 B F20 N3 O2 P Sc |
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Calculated formula | C91 H82 B F20 N3 O2 P Sc |
Title of publication | Scandium complexes containing β-diketiminato ligands with pendant phosphanyl groups: competition between Sc/γ-C [4 + 2] cycloaddition and Sc/P frustrated Lewis pair reactions. |
Authors of publication | Yao, Tu; Xu, Pengfei; Xu, Xin |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2019 |
Journal volume | 48 |
Journal issue | 22 |
Pages of publication | 7743 - 7754 |
a | 12.8116 ± 0.0007 Å |
b | 17.3758 ± 0.0009 Å |
c | 19.3172 ± 0.0008 Å |
α | 94.758 ± 0.004° |
β | 98.99 ± 0.004° |
γ | 98.865 ± 0.004° |
Cell volume | 4171.4 ± 0.4 Å3 |
Cell temperature | 153 ± 2 K |
Ambient diffraction temperature | 153 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.15 |
Residual factor for significantly intense reflections | 0.0792 |
Weighted residual factors for significantly intense reflections | 0.1914 |
Weighted residual factors for all reflections included in the refinement | 0.252 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.028 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7049938.html
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