Crystallography Open Database

Information card for entry 7050284

Preview

Coordinates	7050284.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C60 H144 Cl8 O4 Si8 Sn8
Calculated formula	C60 H144 Cl8 O4 Si8 Sn8
Title of publication	Synthesis and structures of new oligomethylene-bridged double ladders. How far can the layers be separated?
Authors of publication	Jens Beckmann; Dainis Dakternieks; Andrew Duthie; Fong Sheen Kuan; Klaus Jurkschat; Markus Schürman; Edward R. T. Tiekink
Journal of publication	New J.Chem.(Nouv.J.Chim.)
Year of publication	2004
Journal volume	28
Pages of publication	1268 - 1276
a	38.6254 ± 0.0007 Å
b	12.3153 ± 0.0002 Å
c	21.5662 ± 0.0005 Å
α	90°
β	101.392 ± 0.0007°
γ	90°
Cell volume	10056.6 ± 0.3 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.128
Residual factor for significantly intense reflections	0.046
Weighted residual factors for significantly intense reflections	0.051
Weighted residual factors for all reflections included in the refinement	0.063
Goodness-of-fit parameter for all reflections included in the refinement	0.88
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7050284.html