Information card for entry 7050370

Structure parameters

• Formula: C18 H44 N3 O21 P4 Sm
• Calculated formula: C18 H44 N3 O21 P4 Sm
• Title of publication: Complexes of (EtO)2P(O)CH2P(O)(OEt)2 with lanthanide nitrates
• Authors of publication: Lees, Anthony M. J.; Kresinski, Roman A.; Platt, Andrew W. G.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2004
• Journal volume: 28
• Journal issue: 12
• Pages of publication: 1457
• a: 9.63 ± 0.002 Å
• b: 21.727 ± 0.004 Å
• c: 17.275 ± 0.003 Å
• α: 90°
• β: 96.69 ± 0.001°
• γ: 90°
• Cell volume: 3589.9 ± 1.2 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0448
• Residual factor for significantly intense reflections: 0.0429
• Weighted residual factors for significantly intense reflections: 0.1153
• Weighted residual factors for all reflections included in the refinement: 0.1159
• Goodness-of-fit parameter for all reflections included in the refinement: 1.352
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No