Information card for entry 7050504

Structure parameters

• Common name: Samarium(iii) Tris-(Dimethyl-N-trichloroacetylamidophosphate) Complex with 1,10-Phenanthroline
• Chemical name: Samarium(III) Tris-(Dimethyl-N-trichloroacetylamidophosphate) Complex with 1,10-Phenanthroline
• Formula: C24 H26 Cl9 N5 O12 P3 Sm
• Calculated formula: C24 H26 Cl9 N5 O12 P3 Sm
• Title of publication: X-Ray analysis and excited state dynamics in a new class of lanthanide mixed chelates of the type LnPhβ3·Phen (Ln=Sm, Eu, Gd, Tb)
• Authors of publication: Grażyna Oczko; Janina Legendziewicz; Victor Trush; Vladimir Amirkhanov
• Journal of publication: New J. Chem.
• Year of publication: 2003
• Journal volume: 27
• Journal issue: 6
• Pages of publication: 948 - 956
• a: 19.48 ± 0.002 Å
• b: 21.875 ± 0.002 Å
• c: 21.415 ± 0.003 Å
• α: 90°
• β: 109.459 ± 0.008°
• γ: 90°
• Cell volume: 8604.2 ± 1.7 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1317
• Residual factor for significantly intense reflections: 0.0611
• Weighted residual factors for all reflections: 0.1241
• Weighted residual factors for significantly intense reflections: 0.0979
• Goodness-of-fit parameter for all reflections: 1.057
• Goodness-of-fit parameter for significantly intense reflections: 1.158
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No