Information card for entry 7050598

Structure parameters

• Formula: C42 H62 Fe N6 Si2
• Calculated formula: C42 H54 Fe N6 Si2
• Title of publication: Synthesis and structural characterisation of divalent transition metal complexes containing an unsymmetrical benzamidinate ligandElectronic supplementary information (ESI) available: inclination angles in complexes 1?6. See http://www.rsc.org/suppdata/nj/b3/b303527a//
• Authors of publication: Kay Lee, Hung; Suet Lam, Tung; Lam, Chi-Keung; Li, Hung-Wing; Man Fung, Sze
• Journal of publication: New Journal of Chemistry
• Year of publication: 2003
• Journal volume: 27
• Journal issue: 9
• Pages of publication: 1310
• a: 10.414 ± 0.004 Å
• b: 18.633 ± 0.007 Å
• c: 23.86 ± 0.009 Å
• α: 90°
• β: 93.964 ± 0.008°
• γ: 90°
• Cell volume: 4619 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1026
• Residual factor for significantly intense reflections: 0.0503
• Weighted residual factors for significantly intense reflections: 0.134
• Weighted residual factors for all reflections included in the refinement: 0.154
• Goodness-of-fit parameter for all reflections included in the refinement: 0.91
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No