Information card for entry 7050616

Structure parameters

• Common name: [TbCp*2(AMPTMS)]
• Formula: C29 H45 N2 Si Tb
• Calculated formula: C29 H45 N2 Si Tb
• SMILES: [Tb]123456789([n]%10c(N1[Si](C)(C)C)cccc%10C)([c]1([c]9([c]8([c]6([c]51C)C)C)C)C)[c]1([c]3([c]4([c]7([c]21C)C)C)C)C
• Title of publication: Synthesis and structure of the first non ?ate? heteroleptic lanthanoid complexes bearing monoanionic 2-amidopyridine ligands
• Authors of publication: Cole, Marcus L.; Junk, Peter C.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2003
• Journal volume: 27
• Journal issue: 7
• Pages of publication: 1032
• a: 17.207 ± 0.002 Å
• b: 17.207 ± 0.002 Å
• c: 50.082 ± 0.01 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 12842 ± 3 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0359
• Residual factor for significantly intense reflections: 0.0258
• Weighted residual factors for significantly intense reflections: 0.0564
• Weighted residual factors for all reflections included in the refinement: 0.0592
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No