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Information card for entry 7050658
Preview
Coordinates | 7050658.cif |
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Original paper (by DOI) | HTML |
Formula | C138 H192 Ag8 N56 O24 |
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Calculated formula | C148.54 H172 Ag8 N56 O24 |
Title of publication | Synthesis of the silver(i) complex of CH2[CH(pz4Et)2]2 containing the unprecedented [Ag(NO3)4]3? anion: A general method for the preparation of 4-(alkyl)pyrazolesElectronic supplementary information (ESI) available: Crystal packing diagram of the unit cell of [Ag2{�-CH2[CH(pz4Et)2]2}2]3[Ag(NO3)4]2(acetonex/Et2Oy). See http://www.rsc.org/suppdata/nj/b3/b307306h/ |
Authors of publication | Reger, Daniel L.; Gardinier, James R.; Christian Grattan, T.; Smith, Monica R.; Smith, Mark D. |
Journal of publication | New Journal of Chemistry |
Year of publication | 2003 |
Journal volume | 27 |
Journal issue | 11 |
Pages of publication | 1670 |
a | 12.2524 ± 0.0007 Å |
b | 21.8178 ± 0.0013 Å |
c | 27.0779 ± 0.0016 Å |
α | 68.573 ± 0.001° |
β | 80.934 ± 0.001° |
γ | 87.349 ± 0.001° |
Cell volume | 6653.5 ± 0.7 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1109 |
Residual factor for significantly intense reflections | 0.0727 |
Weighted residual factors for significantly intense reflections | 0.2166 |
Weighted residual factors for all reflections included in the refinement | 0.2481 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.028 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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