Information card for entry 7050728

Structure parameters

• Formula: C26 H52 N6 O21 Pb2
• Calculated formula: C26 H50 N6 O21.045 Pb2
• Title of publication: C-Donor lariat ether 'scorpionates'
• Authors of publication: Arya, Pious; Channa, Asif; Cragg, Peter J.; Prince, Paul D.; Steed, Jonathan W.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2002
• Journal volume: 26
• Journal issue: 4
• Pages of publication: 440
• a: 7.6545 ± 0.0005 Å
• b: 12.0537 ± 0.0004 Å
• c: 21.6309 ± 0.0004 Å
• α: 90.671 ± 0.005°
• β: 96.212 ± 0.004°
• γ: 96.61 ± 0.004°
• Cell volume: 1970.28 ± 0.15 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0878
• Residual factor for significantly intense reflections: 0.067
• Weighted residual factors for significantly intense reflections: 0.1733
• Weighted residual factors for all reflections included in the refinement: 0.1892
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No