Information card for entry 7050773

Structure parameters

• Formula: C29 H35 N3 O8 P2 Pd
• Calculated formula: C28 H29 N3 O7 P2 Pd
• Title of publication: Reactivity of a cationic square-planar palladium(II) chloro complex containing bis[2-(diphenylphosphino)ethyl]amine: chloro substitutions by anionic ligands and formation of neutral digold(I) compounds possessing linear PAuX fragments. The X-Ray crystal structure of Au2[Ph2P(CH2)2N(NO)(CH2)2PPh2]Cl2
• Authors of publication: Inés García-Seijo, M.; Habtemariam, Abraha; Parsons, Simon; Gould, R. O.; Esther García-Fernández, M.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2002
• Journal volume: 26
• Journal issue: 5
• Pages of publication: 636
• a: 8.044 ± 0.005 Å
• b: 12.719 ± 0.005 Å
• c: 15.492 ± 0.007 Å
• α: 76.89 ± 0.03°
• β: 82.59 ± 0.04°
• γ: 89.47 ± 0.04°
• Cell volume: 1530.5 ± 1.3 ų
• Cell temperature: 220 ± 2 K
• Ambient diffraction temperature: 220 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0887
• Residual factor for significantly intense reflections: 0.0733
• Weighted residual factors for significantly intense reflections: 0.199
• Weighted residual factors for all reflections included in the refinement: 0.2161
• Goodness-of-fit parameter for all reflections included in the refinement: 1.094
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No