Information card for entry 7050963

Structure parameters

• Formula: C10 H28 Cl N7 Ni O4
• Calculated formula: C10 H28 Cl N7 Ni O4
• Title of publication: Four new NiII antiferromagnetic complexes with azido bridges
• Authors of publication: Montserrat Monfort; Inmaculada Resino; Joan Ribas; Xavier Solans; Mercé Font-Bardia; Helen Stoeckli-Evans
• Journal of publication: New J. Chem.
• Year of publication: 2002
• Journal volume: 26
• Journal issue: 11
• Pages of publication: 1601 - 1606
• a: 8.3715 ± 0.0007 Å
• b: 18.4 ± 0.0012 Å
• c: 12.2042 ± 0.0009 Å
• α: 90°
• β: 95.958 ± 0.01°
• γ: 90°
• Cell volume: 1869.7 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0781
• Residual factor for significantly intense reflections: 0.0381
• Weighted residual factors for significantly intense reflections: 0.0821
• Weighted residual factors for all reflections included in the refinement: 0.0915
• Goodness-of-fit parameter for all reflections included in the refinement: 0.801
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No