Information card for entry 7050965

Structure parameters

• Formula: C16 H32 F6 N7 Ni P
• Calculated formula: C15.61 H35 F3 N7 Ni P
• Title of publication: Four new NiII antiferromagnetic complexes with azido bridges
• Authors of publication: Montserrat Monfort; Inmaculada Resino; Joan Ribas; Xavier Solans; Mercé Font-Bardia; Helen Stoeckli-Evans
• Journal of publication: New J. Chem.
• Year of publication: 2002
• Journal volume: 26
• Journal issue: 11
• Pages of publication: 1601 - 1606
• a: 11.258 ± 0.003 Å
• b: 12.38 ± 0.01 Å
• c: 18.941 ± 0.005 Å
• α: 90°
• β: 103.43 ± 0.02°
• γ: 90°
• Cell volume: 2568 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.219
• Residual factor for significantly intense reflections: 0.0611
• Weighted residual factors for all reflections: 0.2485
• Weighted residual factors for significantly intense reflections: 0.1466
• Goodness-of-fit parameter for all reflections: 1.006
• Goodness-of-fit parameter for significantly intense reflections: 1.137
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No