Information card for entry 7050979

Structure parameters

• Formula: C46 H58 Cl Ge Li N6 O2
• Calculated formula: C46 H58 Cl Ge Li N6 O2
• Title of publication: Diaminocarbene homologues: synthesis and crystal structure of the first diaminogermylene LiCl adduct displaying an electrophilic germanium centre
• Authors of publication: Olaf Kühl; Peter Lönnecke; Joachim Heinicke
• Journal of publication: New J. Chem.
• Year of publication: 2002
• Journal volume: 26
• Journal issue: 10
• Pages of publication: 1304 - 1307
• a: 10.5995 ± 0.0011 Å
• b: 13.3972 ± 0.0014 Å
• c: 17.435 ± 0.0019 Å
• α: 71.24 ± 0.002°
• β: 72.668 ± 0.002°
• γ: 89.64 ± 0.002°
• Cell volume: 2226.9 ± 0.4 ų
• Cell temperature: 218 ± 2 K
• Ambient diffraction temperature: 218 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1298
• Residual factor for significantly intense reflections: 0.053
• Weighted residual factors for significantly intense reflections: 0.092
• Weighted residual factors for all reflections included in the refinement: 0.1123
• Goodness-of-fit parameter for all reflections included in the refinement: 0.882
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No