Information card for entry 7051095

Structure parameters

• Formula: C31 H69 N5 P2
• Calculated formula: C31 H69 N5 P2
• SMILES: P(N(C(C)C)C(C)C)(N(C(C)C)C(C)C)CC(=N\C(C)(C)C)/CP(N(C(C)C)C(C)C)N(C(C)C)C(C)C
• Title of publication: The 'one-pot' syntheses of α,α'-diphosphino-substituted imines: a unique reaction of bulky bis(dialkylamino)chlorophosphines
• Authors of publication: Baceiredo, Antoine; Bertrand, Guy; Dyer, Philip W.; Fawcett, John; Griep-Raming, Nina; Guerret, Olivier; Hanton, Martin J.; Russell, David R.; Williamson, Anna-Maria
• Journal of publication: New Journal of Chemistry
• Year of publication: 2001
• Journal volume: 25
• Journal issue: 4
• Pages of publication: 591
• a: 17.676 ± 0.006 Å
• b: 18.784 ± 0.008 Å
• c: 22.185 ± 0.011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7366 ± 5 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 4
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.163
• Residual factor for significantly intense reflections: 0.0776
• Weighted residual factors for significantly intense reflections: 0.1628
• Weighted residual factors for all reflections included in the refinement: 0.2
• Goodness-of-fit parameter for all reflections included in the refinement: 0.983
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No