Information card for entry 7051139

Structure parameters

• Formula: C30 H27 B Cu F4 N4 O P
• Calculated formula: C30 H27 B Cu F4 N4 O P
• Title of publication: Phosphine oxide functionalised with two bipyridine subunits: a novel ligand for the engineering of sterically hindered complexes
• Authors of publication: Douce, Laurent; Charbonnière, Loïc; Cesario, Michèle; Ziessel, Raymond
• Journal of publication: New Journal of Chemistry
• Year of publication: 2001
• Journal volume: 25
• Journal issue: 8
• Pages of publication: 1024
• a: 7.43 ± 0.003 Å
• b: 14.002 ± 0.005 Å
• c: 15.206 ± 0.006 Å
• α: 114.78 ± 0.02°
• β: 80.67 ± 0.03°
• γ: 98.49 ± 0.03°
• Cell volume: 1411.7 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1109
• Residual factor for significantly intense reflections: 0.0683
• Weighted residual factors for all reflections: 0.1953
• Weighted residual factors for all reflections included in the refinement: 0.1668
• Goodness-of-fit parameter for all reflections: 1.033
• Goodness-of-fit parameter for all reflections included in the refinement: 1.112
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No