Information card for entry 7051163

Structure parameters

• Formula: C36 H48 N2 O6 P4 Pd S2
• Calculated formula: C36 H48 N2 O6 P4 Pd S2
• Title of publication: New mixed-donor unsymmetrical P‒N‒P ligands and their palladium(II) complexes
• Authors of publication: Marek Necas; Mark R. St J. Foreman; Jaromír Marek; J. Derek Woollins; Josef Novosad
• Journal of publication: New J. Chem.
• Year of publication: 2001
• Journal volume: 25
• Journal issue: 10
• Pages of publication: 1256 - 1263
• a: 11.605 ± 0.002 Å
• b: 12.181 ± 0.002 Å
• c: 15.93 ± 0.003 Å
• α: 110.77 ± 0.03°
• β: 91.19 ± 0.03°
• γ: 106.59 ± 0.03°
• Cell volume: 1999.1 ± 0.9 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1212
• Residual factor for significantly intense reflections: 0.0422
• Weighted residual factors for significantly intense reflections: 0.103
• Weighted residual factors for all reflections included in the refinement: 0.122
• Goodness-of-fit parameter for all reflections included in the refinement: 0.982
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No