Information card for entry 7051286

Structure parameters

• Formula: C32 H28.5 Cl4.5 N O P2 Pd
• Calculated formula: C32 H27.5 Cl4.5 N O P2 Pd
• Title of publication: Molybdenum(0), ruthenium(II), palladium(II), platinum(II), copper(I) and gold(I) complexes of a new methoxy functionalised bis(phosphino)amine: synthesis and structure
• Authors of publication: Gaw, Kirsty G.; Smith, Martin B.; Slawin, Alexandra M. Z.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2000
• Journal volume: 24
• Journal issue: 6
• Pages of publication: 429
• a: 11.8731 ± 0.0003 Å
• b: 14.3704 ± 0.0003 Å
• c: 21.5491 ± 0.0005 Å
• α: 90°
• β: 98.502 ± 0.001°
• γ: 90°
• Cell volume: 3636.33 ± 0.15 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1063
• Residual factor for significantly intense reflections: 0.0559
• Weighted residual factors for all reflections: 0.2341
• Weighted residual factors for significantly intense reflections: 0.1564
• Goodness-of-fit parameter for all reflections: 0.849
• Goodness-of-fit parameter for significantly intense reflections: 0.84
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No