Syntheses and crystal structure of [Li4Zn(μ3,η2-ddbfo)2(μ,η2-ddbfo)3Cl(CH3CN)2]·2CH3CN, [Na4(μ,η2-ddbfo)4(CH3CN)4] and [Zn2(μ,η1-ddbfo)2Cl2(py)2] aggregates
Authors of publication
Sobota, Piotr; Klimowicz, Maria; Utko, Józef; Jerzykiewicz, Lucjan B.
Journal of publication
New Journal of Chemistry
Year of publication
2000
Journal volume
24
Journal issue
7
Pages of publication
523
a
9.988 ± 0.002 Å
b
18.643 ± 0.004 Å
c
28.848 ± 0.006 Å
α
84.29 ± 0.03°
β
84.32 ± 0.03°
γ
76 ± 0.03°
Cell volume
5171 ± 2 Å3
Cell temperature
298 ± 1 K
Ambient diffraction temperature
298 ± 1 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0621
Residual factor for significantly intense reflections
0.0395
Weighted residual factors for significantly intense reflections
0.1069
Weighted residual factors for all reflections included in the refinement
0.1183
Goodness-of-fit parameter for all reflections included in the refinement