Information card for entry 7051326

Structure parameters

• Formula: C26 H58 N2 O Os P2
• Calculated formula: C26 H58 N2 O Os P2
• SMILES: [OsH2](N=O)(CC1=NC(CCC1)(C)C)([P](C(C)C)(C(C)C)C(C)C)[P](C(C)C)(C(C)C)C(C)C
• Title of publication: An osmium hydrido methyl species via an unconventional methyl transfer
• Authors of publication: Yandulov, Dmitry V.; Huffman, John C.; Caulton, Kenneth G.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2000
• Journal volume: 24
• Journal issue: 9
• Pages of publication: 649 - 650
• a: 8.833 ± 0.0002 Å
• b: 11.5202 ± 0.0003 Å
• c: 16.055 ± 0.0004 Å
• α: 103.698°
• β: 99.4508 ± 0.0012°
• γ: 98.8901 ± 0.0012°
• Cell volume: 1533.49 ± 0.07 ų
• Cell temperature: 113 K
• Ambient diffraction temperature: 113 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0159
• Weighted residual factors for all reflections included in the refinement: 0.0134
• Goodness-of-fit parameter for all reflections included in the refinement: 0.5487
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No