Information card for entry 7051682

Structure parameters

• Formula: C19 H17 B O10 Os3
• Calculated formula: C19 H17 B O10 Os3
• SMILES: [Os]123([Os]4([Os]1(C#[O])(C#[O])(C#[O])C#[O])(C#[O])(C#[O])(C#[O])[CH](=[CH]4C)B([CH]2=[CH]3C)CCC)(C#[O])(C#[O])C#[O]
• Title of publication: Reactions of H2Os3(CO)10 with triallylboranes: formation of novel triosmium boron-containing olefin clusters
• Authors of publication: Kizas, Ol'ga A.; Erdyakov, Sergey Yu.; Antonov, Dmitrii Yu.; Godovikov, Ivan A.; Vorontsov, Evgenii V.; Dolgushin, Fedor M.; Ezernitskaya, Mariam G.; Barakovskaya, Irina G.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2009
• Journal volume: 33
• Journal issue: 8
• Pages of publication: 1760
• a: 9.5816 ± 0.0007 Å
• b: 28.057 ± 0.002 Å
• c: 9.7448 ± 0.0007 Å
• α: 90°
• β: 114.831 ± 0.001°
• γ: 90°
• Cell volume: 2377.5 ± 0.3 ų
• Cell temperature: 115 ± 2 K
• Ambient diffraction temperature: 115 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0645
• Residual factor for significantly intense reflections: 0.0461
• Weighted residual factors for significantly intense reflections: 0.0972
• Weighted residual factors for all reflections included in the refinement: 0.1018
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No