Information card for entry 7051759

Structure parameters

• Formula: C476 H492 O149 P14 S24 Yb2.33
• Calculated formula: C476 H386 O149 P14 S24 Yb2.34
• Title of publication: Nanoporous materials based on heteroleptic bilayers built up from bisphosphonium, p-sulfonatocalix[4]arene ions
• Authors of publication: Makha, Mohamed; Alias, Yatimah; Raston, Colin L.; Sobolev, Alexandre N.
• Journal of publication: New Journal of Chemistry
• Year of publication: 2008
• Journal volume: 32
• Journal issue: 1
• Pages of publication: 83
• a: 21.256 ± 0.005 Å
• b: 23.536 ± 0.006 Å
• c: 31.09 ± 0.008 Å
• α: 83.291 ± 0.004°
• β: 71.885 ± 0.004°
• γ: 78.756 ± 0.004°
• Cell volume: 14473 ± 6 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.4015
• Residual factor for significantly intense reflections: 0.2119
• Weighted residual factors for significantly intense reflections: 0.4676
• Weighted residual factors for all reflections included in the refinement: 0.5533
• Goodness-of-fit parameter for all reflections included in the refinement: 1.118
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No